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Elemental Analysis
| Elemental Analysis
Price Schedule |
Turnaround Time for all coded with this color is 1 Business Day.
RUSH Requires Advance Notice and 100% Surcharge for a Same Day Turnaround. |
| Carbon, Hydrogen, Nitrogen |
$24 |
| Sulfur |
$22 |
| Chlorine |
$22 |
| Bromine |
$22 |
| Iodine |
$25 |
| Fluorine |
$30 |
| Dried to Constant Weight |
$15 |
| Weight loss on Drying |
$20 |
| Combustion Aids |
$10 |
| Special Combustion Conditions |
$36 |
Turnaround Time for all coded with this color is 3-5 Business Days.
RUSH Requires Advance Notice and 100% Surcharge for a 1-2 Business Day Turnaround. |
| Oxygen, Direct |
$25 |
| Karl Fischer Water (Coulometric) |
$35 |
| Karl Fischer Water (Volumetric) |
Quote |
| pH Determination |
$15 |
| Melting Point (requires 2mg) |
$15 |
| FTIR (requires 1-5 mg) |
$75 |
| UV Scan |
$75 |
| Optical Rotation |
$195 |
| TGA |
$250 |
| Ion Chromatography: |
Single |
| Individual Analytes |
$30 |
| Anion Scan: (F-, Cl-, Br-, NO3-, NO2-, PO4-3, SO4-2) |
$150 |
| Cation Scan: (Li+, Na+, NH4+, K+) |
$125 |
| Inorganic Analysis: |
Sample
Preparation |
Single
Analysis |
| Flame AA |
$40 |
$30 |
| Graphite Furnace AA |
$40 |
$60 |
| ICP |
$40 |
$40 |
| ICP Scan (40-60 Elements) |
No Charge |
$450 |
| ICP-MS |
$60 |
$80 |
| ICP-MS Scan (63 Elements) |
No Charge |
$650 |
| Micro-Ash (not USP) |
– |
$25 |
Turnaround Time for all coded with this color is 10-15 Business Days.
RUSH is subject to Resource Availability for a 5-7 Business Day Turnaround. |
| Gas Chromatography: |
Set-up |
Per Sample |
| 1-3 solvents using the same method |
$1,000 |
$500 |
| 4 or more solvents using the same method |
$1,000 |
$750 |
| GC-Mass Spectroscopy: |
Set-up |
Per Sample |
| Using Client-Provided Method |
$1,500 |
$750 |
| Routine HPLC/IC Analyses: |
Set-up |
Per Sample |
| Methane Sulfonic Acid (MSA) (by IC) |
$1,000 |
$250 |
| Triflouro Acetic Acid (TFA) (by IC) |
$1,000 |
$250 |
| Acetate (OAc) (by HPLC) |
$1,000 |
$250 |
<USP> Analyses: (10 Working-Day Turnaround) |
All USP tests will be performed within a 10 working-day turnaround
(unless performed on a “Rush” basis or part of a quoted project)
“Rush” USP Testing will be quoted on a Time & Materials Basis
|
| Analysis |
Theoretical Range (%) |
Sample
Size (mg) |
Additional Information |
Heavy Metals <231>
Call for Quote
|
10 ppm
20 ppm |
2 grams
1 gram |
This test will only indicate whether or not a metallic impurity, that is colored by sulfide ion, exceeds the Heavy Metals limit. Methods I, II, III are listed in the USP (see below).
QTI performs Method II as default but can also perform Methods I & III (Call for pricing and requirements.)
Substances that typically will respond to this test are lead, mercury, bismuth, arsenic, antimony,tin,
cadmium, silver, copper, and molybdenum |
Residue on Ignition (ROI) <281>
Call for Quote
|
0.1 - 1 |
2 - 3 grams |
All samples which fail to meet monograph specifications will be re-run at $40 per re-fire. |
Karl Fischer <921>
Method Ic Coulumetric
Call for Quote
|
0.1 - 1.0
1.0 - 5.0
> 5.0 |
25 - 50
10 - 20
5 |
Method I (Titrimetric - 1a Direct, 1b Residual, 1c Coulumetric), Method II (Azeotropic), Method III (Gravimetric)
QTI performs Method Method 1c as our default USP analysis
Volumetric Determination Available Under Special Circumstances but must be Quoted by the Lab |
Melting Temperature <741>
Call for Quote
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10 mg |
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Optical Rotation <781>
Call for Quote
|
N/A |
2 - 3 grams |
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IR Spectrophotometric Identification
Call for Quote
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5-10mg |
QTI uses KBr <197K> & Nujol Mull <197M> Sample preparation methods only |
UV <197U>
Call for Quote
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25-50mg |
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LOD <731>
Call for Quote
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1-2 grams |
If it is to constant weight, it will be a minimum of 2 drying times.
Compendial or Non-Compendial = Listed in USP or Not
Compendial = 1 drying time
Non-Compendial = At least 2 drying times
Constant weight is anything <50 mg. We stop once we check and it is <50mg difference from prior drying.
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