Turnaround Time for all coded with this color is 3-5 Business Days.
RUSH Requires Advance Notice and 100% Surcharge for a 1-2 Business Day Turnaround. |
| Oxygen, Direct |
$25 |
| Karl Fischer Water (Coulometric) |
$35 |
| Karl Fischer Water (Volumetric) |
Quote |
| pH Determination |
$15 |
| Melting Point (requires 2mg) |
$15 |
| FTIR (requires 1-5 mg) |
$75 |
| UV Scan |
$75 |
| Optical Rotation |
$195 |
| TGA |
$250 |
| Ion Chromatography: |
Single |
| Individual Analytes |
$30 |
| Anion Scan: (F-, Cl-, Br-, NO3-, NO2-, PO4-3, SO4-2) |
$150 |
| Cation Scan: (Li+, Na+, NH4+, K+) |
$125 |
| Inorganic Analysis: |
Sample
Preparation |
Single
Analysis |
| Flame AA |
$40 |
$30 |
| Graphite Furnace AA |
$40 |
$60 |
| ICP |
$40 |
$40 |
| ICP Scan (40-60 Elements) |
No Charge |
$450 |
| ICP-MS |
$60 |
$80 |
| ICP-MS Scan (63 Elements) |
No Charge |
$650 |
| Micro-Ash (not USP) |
– |
$25 |
<USP> Analyses: (20 Working-Day Turnaround) |
All USP tests will be performed within a 20 working-day turnaround
(unless performed on a “Rush” basis or part of a quoted project)
“Rush” USP Testing will be quoted on a Time & Materials Basis
All non-project related USP test samples must be submitted using a “Request for USP Testing” sheet |
| Analysis |
Theoretical Range (%) |
Sample
Size (mg) |
Additional Information |
Heavy Metals <231>
$300 for Single Determination
$60 per Re-Ashing
|
10 ppm
20 ppm |
2 grams
1 gram |
This test will only indicate whether or not a metallic impurity, that is colored by sulfide ion, exceeds the Heavy Metals limit. Methods I, II, III are listed in the USP (see below).
QTI performs Method II as default but can also perform Methods I & III (Call for pricing and requirements.)
Substances that typically will respond to this test are lead, mercury, bismuth, arsenic, antimony,tin,
cadmium, silver, copper, and molybdenum |
Residue on Ignition (ROI) <281>
$60 for Single Determination
|
0.1 - 1 |
2 - 3 grams |
All samples which fail to meet monograph specifications will be re-run at $40 per re-fire. |
Karl Fischer <921>
Method Ic Coulumetric
$500 Set-up Fee
$150 per Sample
|
0.1 - 1.0
1.0 - 5.0
> 5.0 |
25 - 50
10 - 20
5 |
Method I (Titrimetric - 1a Direct, 1b Residual, 1c Coulumetric), Method II (Azeotropic), Method III (Gravimetric)
QTI performs Method Method 1c as our default USP analysis
Volumetric Determination Available Under Special Circumstances but must be Quoted by the Lab |
Melting Temperature <741>
$500 Set-up Fee
$150 per Sample
|
|
10 mg |
|
Optical Rotation <781>
$500 Set-up Fee
$250 per Sample
|
N/A |
2 - 3 grams |
|
IR Spectrophotometric Identification
$500 Set-up Fee
$250 per Sample
|
|
5-10mg |
QTI uses KBr <197K> & Nujol Mull <197M> Sample preparation methods only |
UV <197U>
$500 Set-up Fee
$250 per Sample
|
|
25-50mg |
|
LOD <731>
$60 per Sample
$40 each additional drying time
|
|
1-2 grams |
If it is to constant weight, it will be a minimum of 2 drying times.
Compendial or Non-Compendial = Listed in USP or Not
Compendial = 1 drying time
Non-Compendial = At least 2 drying times
Constant weight is anything <50 mg. We stop once we check and it is <50mg difference from prior drying.
|
